Information card for entry 7016728

Structure parameters

• Common name: (Ni5(N3)2(3-ClBzO2)4(L)6)(CH2Cl2)4(C4H10O)(H2O)
• Formula: C148 H140 Cl16 N36 Ni10 O30
• Calculated formula: C148 H140 Cl16 N36 Ni10 O30
• Title of publication: Use of 6-methylpyridine-2-carbaldehydeoxime in nickel(ii) carboxylate chemistry: synthetic, structural and magnetic properties of penta and hexanuclear complexes.
• Authors of publication: Escuer, Albert; Vlahopoulou, Gina; Mautner, Franz A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 39
• Pages of publication: 10109 - 10116
• a: 22.7201 ± 0.0007 Å
• b: 24.5465 ± 0.0009 Å
• c: 30.7437 ± 0.0011 Å
• α: 90°
• β: 97.217 ± 0.002°
• γ: 90°
• Cell volume: 17009.9 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1578
• Residual factor for significantly intense reflections: 0.0617
• Weighted residual factors for significantly intense reflections: 0.126
• Weighted residual factors for all reflections included in the refinement: 0.1692
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No