Information card for entry 7016761

Structure parameters

• Formula: C86 H88 Cl2 N2 Pb2 Si2
• Calculated formula: C86 H88 Cl2 N2 Pb2 Si2
• SMILES: c1(c(cc(cc1C(c1ccccc1)c1ccccc1)C)C(c1ccccc1)c1ccccc1)N([Pb]1[Cl][Pb](N(c2c(cc(cc2C(c2ccccc2)c2ccccc2)C)C(c2ccccc2)c2ccccc2)[Si](C)(C)C)[Cl]1)[Si](C)(C)C.c1(ccccc1)C.c1(ccccc1)C
• Title of publication: Extremely bulky amido-group 14 element chloride complexes: Potential synthons for low oxidation state main group chemistry.
• Authors of publication: Li, Jiaye; Stasch, Andreas; Schenk, Christian; Jones, Cameron
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 40
• Pages of publication: 10448 - 10456
• a: 9.8669 ± 0.0004 Å
• b: 13.033 ± 0.0005 Å
• c: 15.5728 ± 0.0007 Å
• α: 79.153 ± 0.002°
• β: 84.525 ± 0.002°
• γ: 72.621 ± 0.002°
• Cell volume: 1875.38 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0559
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0666
• Weighted residual factors for all reflections included in the refinement: 0.0726
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No