Information card for entry 7016994

Structure parameters

• Formula: C88.125 H42.25 B2 Cl0.25 F48 N8 O4 Rh2
• Calculated formula: C88.125 H42.25 B2 Cl0.25 F48 N8 O4 Rh2
• Title of publication: Synthesis and structures of homo- and heterobimetallic rhodium(i) and/or iridium(i) complexes of binucleating bis(1-pyrazolyl)methane ligands.
• Authors of publication: Ho, Joanne H. H.; Wagler, Jörg; Willis, Anthony C.; Messerle, Barbara A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 41
• Pages of publication: 11031 - 11042
• a: 16.1319 ± 0.0003 Å
• b: 19.1238 ± 0.0004 Å
• c: 31.7567 ± 0.0006 Å
• α: 90°
• β: 103.648 ± 0.001°
• γ: 90°
• Cell volume: 9520.4 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0613
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.1069
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No