Information card for entry 7017172

Structure parameters

• Common name: dinitroso((±)-2,7,12-trimethoxy-3,8,13-tris(3-(3- pyridyl)benzoyl)-10,15-dihydro-5H-tribenzo(a,d,g)cyclononane)cobalt(ii) N-methylpyrrolidone clathrate
• Chemical name: dinitroso[(±)-2,7,12-trimethoxy-3,8,13- tris[3-(3-pyridyl)benzoyl]-10,15-dihydro-5H- tribenzo[a,d,g]cyclononane]cobalt(II) N-methylpyrrolidone clathrate
• Formula: C80 H81 Co N9 O19
• Calculated formula: C80 H81 Co N9 O19
• Title of publication: New coordination polymers with extended arm cyclotriguaiacyclene ligands: 1D chains, and interpenetrating or polycatenating 2D (4(2).6(2))(4.6(2))(2) networks.
• Authors of publication: Little, Marc A.; Ronson, Tanya K.; Hardie, Michaele J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 45
• Pages of publication: 12217 - 12227
• a: 11.482 ± 0.002 Å
• b: 15.768 ± 0.003 Å
• c: 23.647 ± 0.004 Å
• α: 78.404 ± 0.007°
• β: 82.58 ± 0.007°
• γ: 76.245 ± 0.006°
• Cell volume: 4058.7 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2794
• Residual factor for significantly intense reflections: 0.1269
• Weighted residual factors for significantly intense reflections: 0.3061
• Weighted residual factors for all reflections included in the refinement: 0.3579
• Goodness-of-fit parameter for all reflections included in the refinement: 1.475
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No