Information card for entry 7017231

Structure parameters

• Formula: C19 H24 Cu2 N10 O12
• Calculated formula: C19 H24 Cu2 N10 O12
• Title of publication: Self assembled tetranuclear Cu(4)(ii), Ni(4)(ii) [2 × 2] square grids and a dicopper(ii) complex of heterocycle based polytopic ligands - Magnetic studies.
• Authors of publication: Mandal, Tarak Nath; Roy, Somnath; Konar, Saugata; Jana, Atanu; Ray, Sangita; Das, Kinsuk; Saha, Rajat; El Fallah, Mohamed Salah; Butcher, Ray J.; Chatterjee, Sudipta; Kar, Susanta Kumar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 44
• Pages of publication: 11866 - 11875
• a: 8.8162 ± 0.0004 Å
• b: 10.299 ± 0.0005 Å
• c: 16.3062 ± 0.0005 Å
• α: 74.779 ± 0.003°
• β: 88.629 ± 0.003°
• γ: 65.135 ± 0.004°
• Cell volume: 1289.86 ± 0.11 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0591
• Residual factor for significantly intense reflections: 0.0345
• Weighted residual factors for significantly intense reflections: 0.0832
• Weighted residual factors for all reflections included in the refinement: 0.0875
• Goodness-of-fit parameter for all reflections included in the refinement: 0.965
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No