Information card for entry 7017504

Structure parameters

• Formula: C45 H47 Cl4 N9 O Pd2
• Calculated formula: C45 H47 Cl4 N9 O Pd2
• Title of publication: Bis-diimidazolylidine complexes of nickel: investigations into nickel catalyzed coupling reactions.
• Authors of publication: Paulose, Tressia A. P.; Wu, Shih-Chang; Olson, Jeremy A.; Chau, Tony; Theaker, Nikki; Hassler, Matt; Quail, J. Wilson; Foley, Stephen R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 1
• Pages of publication: 251 - 260
• a: 30.461 ± 0.002 Å
• b: 7.8144 ± 0.0008 Å
• c: 22.228 ± 0.002 Å
• α: 90°
• β: 120.533 ± 0.004°
• γ: 90°
• Cell volume: 4557.4 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0787
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.0818
• Weighted residual factors for all reflections included in the refinement: 0.0936
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No