Information card for entry 7017507

Structure parameters

• Formula: C34 H51 Cl2 Gd2 N6 Ni2 O28.5
• Calculated formula: C34 H38 Cl2 Gd2 N6 Ni2 O28.5
• Title of publication: Heterometallic cubane-like {M(2)Ln(2)} (M = Ni, Zn; Ln =, Gd, Dy) and {Ni(2)Y(2)} aggregates. Synthesis, structures and magnetic properties.
• Authors of publication: Meng, Zhao-Sha; Guo, Fu-Sheng; Liu, Jun-Liang; Leng, Ji-Dong; Tong, Ming-Liang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 8
• Pages of publication: 2320 - 2329
• a: 13.5287 ± 0.0008 Å
• b: 13.6315 ± 0.0008 Å
• c: 14.4829 ± 0.0008 Å
• α: 87.53 ± 0.002°
• β: 74.001 ± 0.002°
• γ: 77.048 ± 0.002°
• Cell volume: 2501.6 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.111
• Residual factor for significantly intense reflections: 0.0762
• Weighted residual factors for significantly intense reflections: 0.2047
• Weighted residual factors for all reflections included in the refinement: 0.2425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No