Information card for entry 7017510

Structure parameters

• Formula: C40 H58 Cl Dy2 N6 Ni2 O24.5
• Calculated formula: C40 H57 Cl Dy2 N6 Ni2 O24.5
• Title of publication: Heterometallic cubane-like {M(2)Ln(2)} (M = Ni, Zn; Ln =, Gd, Dy) and {Ni(2)Y(2)} aggregates. Synthesis, structures and magnetic properties.
• Authors of publication: Meng, Zhao-Sha; Guo, Fu-Sheng; Liu, Jun-Liang; Leng, Ji-Dong; Tong, Ming-Liang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 8
• Pages of publication: 2320 - 2329
• a: 14.3535 ± 0.0007 Å
• b: 22.2211 ± 0.0011 Å
• c: 17.3358 ± 0.0009 Å
• α: 90°
• β: 99.586 ± 0.001°
• γ: 90°
• Cell volume: 5452.1 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0403
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.094
• Weighted residual factors for all reflections included in the refinement: 0.0968
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No