Crystallography Open Database

Information card for entry 7017615

Preview

Coordinates	7017615.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H34 Bi2 N4 O20
Calculated formula	C26 H34 Bi2 N4 O20
Title of publication	Three novel Bi(iii) complexes with in situ generated anilate ligands: unusual oxidation of cyclohexanedione to dihydroxy benzoquinone.
Authors of publication	Gao, Hui; Zhang, Xian-Ming
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	5
Pages of publication	1562 - 1567
a	9.6935 ± 0.0006 Å
b	10.0302 ± 0.0006 Å
c	11.5844 ± 0.0007 Å
α	65.978 ± 0.001°
β	66.768 ± 0.001°
γ	63.343 ± 0.001°
Cell volume	887.93 ± 0.09 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0332
Residual factor for significantly intense reflections	0.0288
Weighted residual factors for significantly intense reflections	0.0646
Weighted residual factors for all reflections included in the refinement	0.0668
Goodness-of-fit parameter for all reflections included in the refinement	1.085
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7017615.html