Photocrystallographic identification of metastable nitrito linkage isomers in a series of nickel(II) complexes.
Authors of publication
Brayshaw, Simon K.; Easun, Timothy L.; George, Michael W.; Griffin, Alexandra M. E.; Johnson, Andrew L.; Raithby, Paul R.; Savarese, Teresa L.; Schiffers, Stefanie; Warren, John E.; Warren, Mark R.; Teat, Simon J.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2012
Journal volume
41
Journal issue
1
Pages of publication
90 - 97
a
9.672 ± 0.004 Å
b
8.366 ± 0.004 Å
c
11.903 ± 0.005 Å
α
90°
β
108.936 ± 0.006°
γ
90°
Cell volume
911 ± 0.7 Å3
Cell temperature
90 ± 2 K
Ambient diffraction temperature
90 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0567
Residual factor for significantly intense reflections
0.0459
Weighted residual factors for significantly intense reflections
0.1066
Weighted residual factors for all reflections included in the refinement
0.1121
Goodness-of-fit parameter for all reflections included in the refinement
