Information card for entry 7017763

Structure parameters

• Formula: C18 H79 Cl N12 O56 Si6 V17
• Calculated formula: C18 H24 Cl N12 O56 Si6 V17
• Title of publication: Introducing organosilicone source into the synthetic system of polyoxovanadates: two novel {V15Si6O48}-based extended chains.
• Authors of publication: Gao, Yuanzhe; Xu, Yanqing; Cao, Yu; Hu, Changwen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 2
• Pages of publication: 567 - 571
• a: 21.3807 ± 0.0009 Å
• b: 15.2965 ± 0.0007 Å
• c: 22.8517 ± 0.001 Å
• α: 90°
• β: 90.979 ± 0.001°
• γ: 90°
• Cell volume: 7472.6 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0907
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.1634
• Weighted residual factors for all reflections included in the refinement: 0.1932
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No