Information card for entry 7017780

Structure parameters

• Formula: C16 H97 N2 Na8 O164 P5 Pr4 W30
• Calculated formula: C16 H9 N2 Na8 O159.5 P5 Pr4 W30
• Title of publication: New class of Preyssler-lanthanide complexes with modified and extended structures tuned by the lanthanide contraction effect.
• Authors of publication: Qin, Chao; Song, Xue-Zhi; Su, Sheng-Qun; Dang, Song; Feng, Jing; Song, Shu-Yan; Hao, Zhao-Min; Zhang, Hong-Jie
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 8
• Pages of publication: 2399 - 2407
• a: 17.7879 ± 0.0012 Å
• b: 17.98 ± 0.0013 Å
• c: 26.742 ± 0.0018 Å
• α: 88.791 ± 0.001°
• β: 79.049 ± 0.001°
• γ: 71.306 ± 0.001°
• Cell volume: 7946.8 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1324
• Residual factor for significantly intense reflections: 0.0771
• Weighted residual factors for significantly intense reflections: 0.1772
• Weighted residual factors for all reflections included in the refinement: 0.2044
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No