Information card for entry 7017783

Structure parameters

• Formula: C14 H52 N2 Na11 O140 P5 Sm2 W30
• Calculated formula: C14 H6 N2 Na11 O140 P5 Sm2 W30
• Title of publication: New class of Preyssler-lanthanide complexes with modified and extended structures tuned by the lanthanide contraction effect.
• Authors of publication: Qin, Chao; Song, Xue-Zhi; Su, Sheng-Qun; Dang, Song; Feng, Jing; Song, Shu-Yan; Hao, Zhao-Min; Zhang, Hong-Jie
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 8
• Pages of publication: 2399 - 2407
• a: 15.685 ± 0.0014 Å
• b: 15.719 ± 0.0014 Å
• c: 17.2013 ± 0.0015 Å
• α: 67.211 ± 0.001°
• β: 65.172 ± 0.001°
• γ: 83.081 ± 0.002°
• Cell volume: 3544.1 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1328
• Residual factor for significantly intense reflections: 0.1155
• Weighted residual factors for significantly intense reflections: 0.2695
• Weighted residual factors for all reflections included in the refinement: 0.2792
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No