Information card for entry 7017834

Structure parameters

• Formula: C46 H77 N3 O P3 Y
• Calculated formula: C46 H77 N3 O P3 Y
• Title of publication: Synthesis and characterization of organo-scandium and yttrium complexes stabilized by phosphinoamide ligands.
• Authors of publication: Halcovitch, Nathan R.; Fryzuk, Michael D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 5
• Pages of publication: 1524 - 1528
• a: 17.026 ± 0.0009 Å
• b: 13.4302 ± 0.0006 Å
• c: 23.0701 ± 0.0013 Å
• α: 90°
• β: 104.733 ± 0.001°
• γ: 90°
• Cell volume: 5101.8 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0463
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections included in the refinement: 0.0908
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No