Information card for entry 7017847

Structure parameters

• Formula: C234 H310 N36 O292 Sb6 V19 W66
• Calculated formula: C234 H306 N36 O292 Sb6 V19 W66
• Title of publication: Novel hexagonal {V=O}6-containing sandwich-type cluster accompanied by in situ carbon-carbon bond formation of organic cations.
• Authors of publication: Han, Zhangang; Zhang, Qixia; Gao, Yuanzhe; Wu, Jingjing; Zhai, Xueliang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 4
• Pages of publication: 1332 - 1337
• a: 49.204 ± 0.002 Å
• b: 49.204 ± 0.002 Å
• c: 15.0273 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 31507 ± 2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0686
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for significantly intense reflections: 0.1419
• Weighted residual factors for all reflections included in the refinement: 0.1546
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No