Information card for entry 7017966

Structure parameters

• Formula: C52 H80 N4 Pb2 Si2
• Calculated formula: C52 H80 N4 Pb2 Si2
• SMILES: [Pb]12N(c3c(cccc3C(C)C)C(C)C)[Si](C)(C)[N]1(c1c(cccc1C(C)C)C(C)C)[Pb]1N(c3c(cccc3C(C)C)C(C)C)[Si](C)(C)[N]12c1c(cccc1C(C)C)C(C)C
• Title of publication: Synthesis and structural characterization of two-coordinate low-valent 14-group metal complexes bearing bulky bis(amido)silane ligands.
• Authors of publication: Yang, Dongming; Guo, Jianmei; Wu, Haishun; Ding, Yuqiang; Zheng, Wenjun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 7
• Pages of publication: 2187 - 2194
• a: 12.444 ± 0.004 Å
• b: 18.724 ± 0.006 Å
• c: 12.638 ± 0.004 Å
• α: 90°
• β: 116.42 ± 0.004°
• γ: 90°
• Cell volume: 2637.1 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0403
• Residual factor for significantly intense reflections: 0.0259
• Weighted residual factors for significantly intense reflections: 0.0562
• Weighted residual factors for all reflections included in the refinement: 0.0593
• Goodness-of-fit parameter for all reflections included in the refinement: 0.944
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No