Information card for entry 7018238

Structure parameters

• Formula: C31 H46 B2 N4
• Calculated formula: C31 H46 B2 N4
• Title of publication: Synthesis and solvent dependent reactivity of chelating bis-N-heterocyclic carbene complexes of Fe((II)) hydrides.
• Authors of publication: Zlatogorsky, Sergey; Ingleson, Michael J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 9
• Pages of publication: 2685 - 2693
• a: 19.641 ± 0.006 Å
• b: 13.9423 ± 0.0016 Å
• c: 16.592 ± 0.005 Å
• α: 90°
• β: 135.8 ± 0.06°
• γ: 90°
• Cell volume: 3168 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1627
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.1513
• Weighted residual factors for all reflections included in the refinement: 0.181
• Goodness-of-fit parameter for all reflections included in the refinement: 0.878
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No