Information card for entry 7018365

Structure parameters

• Chemical name: 1,2-bis(benzoquinoline imine) cyclohexane Ni I2, dichloromethane
• Formula: C36.65 H33.3 Cl7.15 I2.15 N4 Ni2
• Calculated formula: C36.65 H33.3 Cl7.145 I2.155 N4 Ni2
• Title of publication: Mono- and dinuclear nickel(ii) complexes of resolved Schiff-base ligands with extended quinoline substituents.
• Authors of publication: Prema, Dipesh; Oshin, Kayode; Desper, John; Levy, Christopher J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 16
• Pages of publication: 4998 - 5009
• a: 13.8504 ± 0.0014 Å
• b: 14.2408 ± 0.0015 Å
• c: 23.225 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4580.9 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1935
• Residual factor for significantly intense reflections: 0.0784
• Weighted residual factors for significantly intense reflections: 0.1883
• Weighted residual factors for all reflections included in the refinement: 0.2287
• Goodness-of-fit parameter for all reflections included in the refinement: 0.974
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No