Information card for entry 7018373

Structure parameters

• Formula: C174 H178 Cl9 Eu3 N36 O47
• Calculated formula: C174 H144 Cl9 Eu3 N36 O47
• Title of publication: Metal induced folding: synthesis and conformational analysis of the lanthanide complexes of two 44-membered hydrazone macrocycles.
• Authors of publication: Klein, Jörg M; Clegg, Jack K.; Saggiomo, Vittorio; Reck, Lisa; Lüning, Ulrich; Sanders, Jeremy K. M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 13
• Pages of publication: 3780 - 3786
• a: 15.344 ± 0.003 Å
• b: 22.768 ± 0.005 Å
• c: 36.352 ± 0.007 Å
• α: 79.55 ± 0.03°
• β: 87.57 ± 0.03°
• γ: 76.21 ± 0.03°
• Cell volume: 12129 ± 5 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1766
• Residual factor for significantly intense reflections: 0.0951
• Weighted residual factors for significantly intense reflections: 0.2745
• Weighted residual factors for all reflections included in the refinement: 0.3112
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No