Information card for entry 7018579

Structure parameters

• Formula: C23 H34 Br2 N2 Si Zn
• Calculated formula: C23 H34 Br2 N2 Si Zn
• SMILES: Br[Zn]1(Br)[N](C)(C)[C@@H]2CCCC[C@H]2[N]1(C)C[Si](C)(c1ccccc1)c1ccccc1
• Title of publication: Preparation of aminomethyl functionalised silanes via an α-lithiated amine: From their synthesis, stability and crystal structures to stereochemical issues.
• Authors of publication: Gessner, Viktoria H.; Strohmann, Carsten
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 12
• Pages of publication: 3452 - 3460
• a: 12.3467 ± 0.0006 Å
• b: 11.0348 ± 0.0006 Å
• c: 19.5297 ± 0.0014 Å
• α: 90°
• β: 106.652 ± 0.007°
• γ: 90°
• Cell volume: 2549.2 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.0674
• Weighted residual factors for all reflections included in the refinement: 0.0691
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No