Information card for entry 7018581

Structure parameters

• Formula: C18 H32 Cl2 N2 Si Zn
• Calculated formula: C18 H32 Cl2 N2 Si Zn
• SMILES: C[N]1(C)[C@@H]2CCCC[C@H]2[N](C)(C[Si](C)(C)c2ccccc2)[Zn]1(Cl)Cl
• Title of publication: Preparation of aminomethyl functionalised silanes via an α-lithiated amine: From their synthesis, stability and crystal structures to stereochemical issues.
• Authors of publication: Gessner, Viktoria H.; Strohmann, Carsten
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 12
• Pages of publication: 3452 - 3460
• a: 11.3678 ± 0.0013 Å
• b: 8.2162 ± 0.0009 Å
• c: 11.6616 ± 0.0017 Å
• α: 90°
• β: 95.005 ± 0.013°
• γ: 90°
• Cell volume: 1085 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1327
• Residual factor for significantly intense reflections: 0.0709
• Weighted residual factors for significantly intense reflections: 0.1271
• Weighted residual factors for all reflections included in the refinement: 0.1384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No