Information card for entry 7018585

Structure parameters

• Formula: C52 H72 N4
• Calculated formula: C52 H58 N4
• Title of publication: Reduction of Sterically Hindered β-Diketiminato Europium(iii) Complexes by the β-Diketiminato Anion: A Convenient Route for the Synthesis of β-Diketiminato Europium(ii) Complexes.
• Authors of publication: Shen, Xiaodong; Zhang, Yong; Xue, Mingqiang; Shen, Qi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 13
• Pages of publication: 3668 - 3674
• a: 8.566 ± 0.004 Å
• b: 9.953 ± 0.005 Å
• c: 15.152 ± 0.006 Å
• α: 100.318 ± 0.009°
• β: 90.767 ± 0.008°
• γ: 113.822 ± 0.016°
• Cell volume: 1157.4 ± 0.9 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2176
• Residual factor for significantly intense reflections: 0.1067
• Weighted residual factors for significantly intense reflections: 0.2291
• Weighted residual factors for all reflections included in the refinement: 0.2896
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No