Crystallography Open Database

Information card for entry 7018588

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Structure parameters

Formula	C23 H30 N2
Calculated formula	C23 H30 N2
SMILES	N(C(/C)=C\C(=N\c1ccccc1)\C)c1c(cccc1C(C)C)C(C)C
Title of publication	Reduction of Sterically Hindered β-Diketiminato Europium(iii) Complexes by the β-Diketiminato Anion: A Convenient Route for the Synthesis of β-Diketiminato Europium(ii) Complexes.
Authors of publication	Shen, Xiaodong; Zhang, Yong; Xue, Mingqiang; Shen, Qi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	13
Pages of publication	3668 - 3674
a	9.65 ± 0.004 Å
b	11.038 ± 0.005 Å
c	11.101 ± 0.005 Å
α	112.159 ± 0.007°
β	97.821 ± 0.007°
γ	102.366 ± 0.005°
Cell volume	1038.5 ± 0.8 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1112
Residual factor for significantly intense reflections	0.0865
Weighted residual factors for significantly intense reflections	0.269
Weighted residual factors for all reflections included in the refinement	0.2951
Goodness-of-fit parameter for all reflections included in the refinement	1.169
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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