Information card for entry 7018604

Structure parameters

• Formula: C14 H45 N3 O46.5 P Tm2 W10
• Calculated formula: C14 H36 N3 O46.5 P Tm2 W10
• Title of publication: Two types of oxalate-bridging rare-earth-substituted Keggin-type phosphotungstates {[(α-PW(11)O(39))RE(H(2)O)](2)(C(2)O(4))}(10-) and {(α-x-PW(10)O(38))RE(2)(C(2)O(4))(H(2)O)(2)}(3-).
• Authors of publication: Zhang, Shaowei; Wang, Yuan; Zhao, Junwei; Ma, Pengtao; Wang, Jingping; Niu, Jingyang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 13
• Pages of publication: 3764 - 3772
• a: 20.517 ± 0.011 Å
• b: 18.239 ± 0.009 Å
• c: 18.608 ± 0.009 Å
• α: 90°
• β: 102.65 ± 0.01°
• γ: 90°
• Cell volume: 6794 ± 6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1068
• Residual factor for significantly intense reflections: 0.0665
• Weighted residual factors for significantly intense reflections: 0.1902
• Weighted residual factors for all reflections included in the refinement: 0.2124
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No