Information card for entry 7018725

Structure parameters

• Formula: C16 H6 Cl2 F12 Ge
• Calculated formula: C16 H6 Cl2 F12 Ge
• Title of publication: Synthesis and characterisation of selected group 14 derivatives of the 2,5-(CF(3))(2)C(6)H(3) (Ar) ligand.
• Authors of publication: Coffer, Philippa K.; Dillon, Keith B.; Howard, Judith A. K.; Yufit, Dmitry S.; Zorina, Natalia V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 15
• Pages of publication: 4460 - 4468
• a: 9.7607 ± 0.0003 Å
• b: 12.0194 ± 0.0004 Å
• c: 16.2537 ± 0.0005 Å
• α: 76.83 ± 0.01°
• β: 89.82 ± 0.02°
• γ: 86.76 ± 0.01°
• Cell volume: 1853.63 ± 0.13 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1119
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1042
• Weighted residual factors for all reflections included in the refinement: 0.1191
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No