Information card for entry 7018939

Structure parameters

• Formula: C30 H24 As P S
• Calculated formula: C30 H24 As P S
• SMILES: [As](Sc1c(P(c2ccccc2)c2ccccc2)cccc1)(c1ccccc1)c1ccccc1
• Title of publication: Reaction of a heterotopic P,SAs ligand with group 10 metal(ii) complexes: As-S bond cleavage and the formation of two unusual trinuclear structural isomers for Pd and Pt.
• Authors of publication: Sárosi, Imola; Hildebrand, Alexandra; Lönnecke, Peter; Silaghi-Dumitrescu, Luminiţa; Hey-Hawkins, Evamarie
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 17
• Pages of publication: 5326 - 5333
• a: 10.483 ± 0.0002 Å
• b: 9.8797 ± 0.0003 Å
• c: 48.4808 ± 0.0013 Å
• α: 90°
• β: 93.39 ± 0.002°
• γ: 90°
• Cell volume: 5012.3 ± 0.2 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0989
• Residual factor for significantly intense reflections: 0.0721
• Weighted residual factors for significantly intense reflections: 0.13
• Weighted residual factors for all reflections included in the refinement: 0.1355
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No