Synthesis, structure, properties and immobilization on a gold surface of the monoribbed-functionalized tris-dioximate cobalt(ii) clathrochelates and an electrocatalytic hydrogen production from H+ ions
Authors of publication
Voloshin, Y. Z.; Belov, A. S.; Vologzhanina, A. V.; Aleksandrov, G. G.; Dolganov, A. V.; Novikov, V. V.; Varzatskii, O. A.; Bubnov, Y. N.
Journal of publication
Dalton Transactions
Year of publication
2012
Journal volume
41
Journal issue
20
Pages of publication
6078
a
13.5294 ± 0.0011 Å
b
17.7456 ± 0.0015 Å
c
16.38 ± 0.0013 Å
α
90°
β
94.896 ± 0.002°
γ
90°
Cell volume
3918.3 ± 0.6 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
8
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.1187
Residual factor for significantly intense reflections
0.0485
Weighted residual factors for significantly intense reflections
0.0703
Weighted residual factors for all reflections included in the refinement
0.0782
Goodness-of-fit parameter for all reflections included in the refinement
