Information card for entry 7019125

Structure parameters

• Formula: C20 H32 Br4 N4 Ni2
• Calculated formula: C20 H32 Br4 N4 Ni2
• SMILES: c1cccc2CC[NH]([Ni]3([n]12)(Br)[Br][Ni]1([n]2ccccc2CC[NH]1C(C)C)([Br]3)Br)C(C)C
• Title of publication: Synthesis, structures of (aminopyridine)nickel complexes and their use for catalytic ethylene polymerization.
• Authors of publication: Lin, Ya-Chi; Yu, Kuo-Hsuan; Lin, Ya-Fan; Lee, Gene-Hsiang; Wang, Yu; Liu, Shiuh-Tzung; Chen, Jwu-Ting
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 22
• Pages of publication: 6661 - 6670
• a: 8.0121 ± 0.0003 Å
• b: 8.6141 ± 0.0003 Å
• c: 10.4721 ± 0.0004 Å
• α: 76.293 ± 0.001°
• β: 89.199 ± 0.001°
• γ: 71.404 ± 0.001°
• Cell volume: 664.02 ± 0.04 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0338
• Residual factor for significantly intense reflections: 0.0225
• Weighted residual factors for significantly intense reflections: 0.0508
• Weighted residual factors for all reflections included in the refinement: 0.0529
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No