Information card for entry 7019265

Structure parameters

• Formula: C51.6 H109.2 Cl1.6 Dy4 Mn4 N13.2 O44
• Calculated formula: C51.6 H98 Cl1.6 Dy4 Mn4 N13.2 O44
• Title of publication: Using the flexible ligand bis(2-hydroxyethyl)amino-tris (hydroxymethyl)methane ("bis-tris") to access a family of 3d-4f Mn(III)(4)Ln(4) complexes.
• Authors of publication: Khan, Amin; Lan, Yanhua; Kostakis, George E.; Anson, Christopher E.; Powell, Annie K.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 27
• Pages of publication: 8333 - 8339
• a: 11.2153 ± 0.0008 Å
• b: 13.7027 ± 0.001 Å
• c: 14.3792 ± 0.001 Å
• α: 106.212 ± 0.006°
• β: 92.408 ± 0.006°
• γ: 98.372 ± 0.006°
• Cell volume: 2091.3 ± 0.3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0954
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1322
• Weighted residual factors for all reflections included in the refinement: 0.1469
• Goodness-of-fit parameter for all reflections included in the refinement: 0.95
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No