Information card for entry 7019287

Structure parameters

• Common name: Cr2Co(dpa)4(N3)2(Et2O)
• Formula: C44 H42 Co Cr2 N18 O
• Calculated formula: C44 H42 Co Cr2 N18 O
• Title of publication: Synthesis, characterization and thermal properties of trimetallic N(3)-Cr[quadruple bond, length as m-dash]CrM-N(3) azide complexes with M = Cr, Mn, Fe, and Co.
• Authors of publication: Turov, Yevgeniya; Berry, John F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 26
• Pages of publication: 8153 - 8161
• a: 15.902 ± 0.0003 Å
• b: 16.1624 ± 0.0003 Å
• c: 17.5796 ± 0.0003 Å
• α: 90°
• β: 104.688 ± 0.001°
• γ: 90°
• Cell volume: 4370.56 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0427
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0843
• Weighted residual factors for all reflections included in the refinement: 0.09
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No