Information card for entry 7019629

Structure parameters

• Formula: C59 H62 Ag2 Cl6 N4 O17 P4
• Calculated formula: C59 H62 Ag2 Cl6 N4 O17 P4
• SMILES: [Ag]1([P](CN2CC[N+](=C2)C[P]([Ag]([P](CN2CC[N+](=C2)C[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)OCl(=O)(=O)=O)(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)OCl(=O)(=O)=O.Cl(=O)(=O)(=O)[O-].Cl(=O)(=O)(=O)[O-].C(Cl)Cl.O
• Title of publication: Formation of N-heterocyclic diphosphine ligands from Ag(i)-assisted condensation reactions between bdppeda and formaldehyde and their binuclear silver(i) complexes.
• Authors of publication: Sun, Sha; Ren, Zhi-Gang; Yang, Ju-Hua; He, Run-Tian; Wang, Fan; Wu, Xin-Yi; Gong, Wei-Jie; Li, Hong-Xi; Lang, Jian-Ping
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 27
• Pages of publication: 8447 - 8454
• a: 24.496 ± 0.005 Å
• b: 15.496 ± 0.003 Å
• c: 19.454 ± 0.004 Å
• α: 90°
• β: 112.31 ± 0.03°
• γ: 90°
• Cell volume: 6832 ± 3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.159
• Residual factor for significantly intense reflections: 0.115
• Weighted residual factors for significantly intense reflections: 0.1837
• Weighted residual factors for all reflections included in the refinement: 0.2029
• Goodness-of-fit parameter for all reflections included in the refinement: 1.232
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No