Information card for entry 7019667

Structure parameters

• Formula: C82.4 H93.6 B4 Co4 F20 N16 O2.4
• Calculated formula: C82.4 H93.6 B4 Co4 F20 N16 O2.4
• Title of publication: Solvent control: dinuclear versus tetranuclear complexes of a bis-tetradentate pyrimidine-based ligand.
• Authors of publication: Gobeze, Worku A.; Milway, Victoria A.; Moubaraki, Boujemaa; Murray, Keith S.; Brooker, Sally
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 32
• Pages of publication: 9708 - 9721
• a: 14.8889 ± 0.0013 Å
• b: 22.663 ± 0.002 Å
• c: 26.145 ± 0.002 Å
• α: 90°
• β: 102.529 ± 0.004°
• γ: 90°
• Cell volume: 8611.9 ± 1.3 ų
• Cell temperature: 91 ± 2 K
• Ambient diffraction temperature: 91 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0424
• Residual factor for significantly intense reflections: 0.0375
• Weighted residual factors for significantly intense reflections: 0.0964
• Weighted residual factors for all reflections included in the refinement: 0.0994
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No