Crystallography Open Database

Information card for entry 7019673

7019672 << 7019673 >> 7019674

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Coordinates	7019673.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H70 Cl2 N9 Ni6 O60 P W9
Calculated formula	C18 H48 Cl2 N9 Ni6 O52 P W9
Title of publication	Assembly of an undeca-nuclear nickel substituted POM through polycarboxylate ligand.
Authors of publication	Zheng, Yun-Yun; Wen, Ru; Kong, Xiang-Jian; Long, La-Sheng; Huang, Rong-Bin; Zheng, Lan-Sun
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	33
Pages of publication	9871 - 9875
a	19.698 ± 0.0005 Å
b	19.0319 ± 0.0005 Å
c	20.2888 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	7606.1 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	36
Hermann-Mauguin space group symbol	C m c 21
Hall space group symbol	C 2c -2
Residual factor for all reflections	0.0516
Residual factor for significantly intense reflections	0.0456
Weighted residual factors for significantly intense reflections	0.0912
Weighted residual factors for all reflections included in the refinement	0.0943
Goodness-of-fit parameter for all reflections included in the refinement	1.001
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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