Information card for entry 7019687

Structure parameters

• Formula: C44 H52.5 Al F N O P
• Calculated formula: C44 H52.5 Al F N O P
• Title of publication: Dimeric aluminum-phosphorus compounds as masked frustrated Lewis pairs for small molecule activation.
• Authors of publication: Roters, Steffi; Appelt, Christian; Westenberg, Hauke; Hepp, Alexander; Slootweg, J. Chris; Lammertsma, Koop; Uhl, Werner
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 30
• Pages of publication: 9033 - 9045
• a: 38.2157 ± 0.0004 Å
• b: 14.1078 ± 0.0001 Å
• c: 15.6568 ± 0.0002 Å
• α: 90°
• β: 112.305 ± 0.001°
• γ: 90°
• Cell volume: 7809.6 ± 0.15 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1546
• Weighted residual factors for all reflections included in the refinement: 0.161
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No