Information card for entry 7019829

Structure parameters

• Formula: C16 H21 Ga N
• Calculated formula: C16 H21 Ga N
• Title of publication: Intramolecular Lewis acid-base pairs based on 4-ethynyl-2,6-lutidine.
• Authors of publication: Winkelhaus, Daniel; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 30
• Pages of publication: 9143 - 9150
• a: 24.6455 ± 0.001 Å
• b: 15.594 ± 0.0007 Å
• c: 17.8708 ± 0.0008 Å
• α: 90°
• β: 119.238 ± 0.002°
• γ: 90°
• Cell volume: 5993.1 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0888
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.0853
• Weighted residual factors for all reflections included in the refinement: 0.0995
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No