Information card for entry 7019912

Structure parameters

• Formula: C38 H94 Mo8 N6 O26
• Calculated formula: C38 H94 Mo8 N6 O28
• Title of publication: Mapping the synthesis of low nuclearity polyoxometalates from octamolybdates to Mn-Anderson clusters.
• Authors of publication: Rosnes, Mali H.; Yvon, Carine; Long, De-Liang; Cronin, Leroy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 33
• Pages of publication: 10071 - 10079
• a: 12.6794 ± 0.0007 Å
• b: 11.9967 ± 0.0006 Å
• c: 20.892 ± 0.0011 Å
• α: 90°
• β: 95.176 ± 0.003°
• γ: 90°
• Cell volume: 3164.9 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0393
• Residual factor for significantly intense reflections: 0.0286
• Weighted residual factors for significantly intense reflections: 0.0687
• Weighted residual factors for all reflections included in the refinement: 0.076
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No