Information card for entry 7020004

Structure parameters

• Formula: C40 H218 Cu10 Ge4 K4 N40 O184 Pr2 W44
• Calculated formula: C40 H160 Cu10 Ge4 K4 N40 O184 Pr2 W44
• Title of publication: Novel polyoxometalate hybrids consisting of copper-lanthanide heterometallic/lanthanide germanotungstate fragments.
• Authors of publication: Zhao, Junwei; Shi, Dongying; Chen, Lijuan; Li, Yanzhou; Ma, Pengtao; Wang, Jingping; Niu, Jingyang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 35
• Pages of publication: 10740 - 10751
• a: 23.046 ± 0.003 Å
• b: 20.377 ± 0.003 Å
• c: 26.318 ± 0.004 Å
• α: 90°
• β: 94.774 ± 0.003°
• γ: 90°
• Cell volume: 12316 ± 3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0809
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.0945
• Weighted residual factors for all reflections included in the refinement: 0.1026
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No