Information card for entry 7020033

Structure parameters

• Common name: [Dy14(CO3)13(ccnm)10(OH)(H2O)6(phen)13](phen).5
• Chemical name: [Dy14(CO3)13(ccnm)10(OH)(H2O)6(phen)13](phen).5
• Formula: C205 H141 Dy14 N57 O66
• Calculated formula: C205 H128 Dy14 N57 O66
• Title of publication: Tetradecanuclear polycarbonatolanthanoid clusters: Diverse coordination modes of carbonate providing access to novel core geometries.
• Authors of publication: Chesman, Anthony S. R.; Turner, David R.; Moubaraki, Boujemaa; Murray, Keith S.; Deacon, Glen B.; Batten, Stuart R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 36
• Pages of publication: 10903 - 10909
• a: 70.91 ± 0.014 Å
• b: 22.072 ± 0.004 Å
• c: 39.35 ± 0.008 Å
• α: 90°
• β: 112.57 ± 0.03°
• γ: 90°
• Cell volume: 56871 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.162
• Weighted residual factors for all reflections included in the refinement: 0.1691
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.77371 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No