Information card for entry 7020112

Structure parameters

• Common name: bis-(Triphenylarsine)dinitro-palladium(II)
• Formula: C36 H30 As2 N2 O4 Pd
• Calculated formula: C36 H30 As2 N2.002 O4.004 Pd
• Title of publication: Photoactivated linkage isomerism in single crystals of nickel, palladium and platinum di-nitro complexes - a photocrystallographic investigation.
• Authors of publication: Warren, Mark R.; Brayshaw, Simon K.; Hatcher, Lauren E.; Johnson, Andrew L.; Schiffers, Stefanie; Warren, Anna J.; Teat, Simon J.; Warren, John E.; Woodall, Christopher H.; Raithby, Paul R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 42
• Pages of publication: 13173 - 13179
• a: 9.5967 ± 0.0009 Å
• b: 9.9479 ± 0.0009 Å
• c: 10.1121 ± 0.0009 Å
• α: 111.262 ± 0.001°
• β: 90.931 ± 0.001°
• γ: 114.454 ± 0.001°
• Cell volume: 803.05 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0397
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.1032
• Weighted residual factors for all reflections included in the refinement: 0.1061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.7749 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No