Information card for entry 7020290

Structure parameters

• Formula: C48 H60 Cl4 N6 Pd2
• Calculated formula: C48 H60 Cl4 N6 Pd2
• Title of publication: Synthesis and characterization of dinuclear NHC-palladium complexes and their applications in the Hiyama reactions of aryltrialkyoxysilanes with aryl chlorides.
• Authors of publication: Yang, Jin; Wang, Lei
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 39
• Pages of publication: 12031 - 12037
• a: 19.2748 ± 0.0005 Å
• b: 19.2748 ± 0.0005 Å
• c: 13.3673 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4966.2 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0898
• Residual factor for significantly intense reflections: 0.0504
• Weighted residual factors for significantly intense reflections: 0.0967
• Weighted residual factors for all reflections included in the refinement: 0.111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No