Information card for entry 7020416

Structure parameters

• Formula: C83 H92 Fe6 N2 O6 P2
• Calculated formula: C83 H92 Fe6 N2 O6 P2
• Title of publication: Reactions of the phosphinidene-bridged complexes [Fe(2)(η(5)-C(5)H(5))(2)(μ-PR)(μ-CO)(CO)(2)] (R = Cy, Ph) with electrophiles based on p-block elements.
• Authors of publication: Alvarez, M. Angeles; García, M Esther; González, Rocío; Ruiz, Miguel A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 48
• Pages of publication: 14498 - 14513
• a: 25.7535 ± 0.0005 Å
• b: 15.5862 ± 0.0004 Å
• c: 19.4501 ± 0.0003 Å
• α: 90°
• β: 111.956 ± 0.001°
• γ: 90°
• Cell volume: 7241 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0569
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.135
• Weighted residual factors for all reflections included in the refinement: 0.1563
• Goodness-of-fit parameter for all reflections included in the refinement: 1.108
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No