Information card for entry 7020446

Structure parameters

• Formula: C70 H74 N6 O9 Re2 Si2
• Calculated formula: C70 H74 N6 O9 Re2 Si2
• Title of publication: The group 7 metal carbonyl complexes from a stable heteroleptic silylene PhC(NtBu)2SiNPh2.
• Authors of publication: Azhakar, Ramachandran; Roesky, Herbert W.; Holstein, Julian J.; Dittrich, Birger
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 39
• Pages of publication: 12096 - 12100
• a: 13.3137 ± 0.0003 Å
• b: 24.3365 ± 0.0005 Å
• c: 20.8196 ± 0.0004 Å
• α: 90°
• β: 95.935 ± 0.001°
• γ: 90°
• Cell volume: 6709.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0463
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.1413
• Weighted residual factors for all reflections included in the refinement: 0.1415
• Goodness-of-fit parameter for all reflections included in the refinement: 1.241
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No