Crystallography Open Database

Information card for entry 7020635

7020634 << 7020635 >> 7020636

Preview

Coordinates	7020635.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C95.6 H128.4 F12 N12 O18.6 Rh4 S4
Calculated formula	C87.6 H107.4 F12 N12 O16.6 Rh4 S4
Title of publication	Stepwise formation of organometallic macrocycles and triangular prisms containing 2,2'-bisbenzimidazole ligands.
Authors of publication	Wu, Tong; Lin, Yue-Jian; Jin, Guo-Xin
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	1
Pages of publication	82 - 88
a	13.3751 ± 0.0008 Å
b	32.7892 ± 0.0018 Å
c	14.0292 ± 0.0008 Å
α	90°
β	116.633 ± 0.001°
γ	90°
Cell volume	5499.8 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0773
Residual factor for significantly intense reflections	0.0496
Weighted residual factors for significantly intense reflections	0.1281
Weighted residual factors for all reflections included in the refinement	0.1395
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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