Information card for entry 7020637

Structure parameters

• Formula: C129 H136 Ag F15 Ir4 N16 O19 S5
• Calculated formula: C116 H104 Ag F12 Ir4 N16 O13 S4
• Title of publication: Stepwise formation of organometallic macrocycles and triangular prisms containing 2,2'-bisbenzimidazole ligands.
• Authors of publication: Wu, Tong; Lin, Yue-Jian; Jin, Guo-Xin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 1
• Pages of publication: 82 - 88
• a: 33.945 ± 0.002 Å
• b: 25.8578 ± 0.0018 Å
• c: 28.822 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 25298 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.1257
• Residual factor for significantly intense reflections: 0.0723
• Weighted residual factors for significantly intense reflections: 0.1869
• Weighted residual factors for all reflections included in the refinement: 0.2118
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No