Information card for entry 7020692

Structure parameters

• Formula: C47 H78 N5 O Si4 U
• Calculated formula: C47 H78 N5 O Si4 U
• Title of publication: Carbon monoxide and carbon dioxide insertion chemistry of f-block N-heterocyclic carbene complexes.
• Authors of publication: Arnold, Polly L.; Turner, Zöe R; Germeroth, Anne I.; Casely, Ian J.; Nichol, Gary S.; Bellabarba, Ronan; Tooze, Robert P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 5
• Pages of publication: 1333 - 1337
• a: 13.3289 ± 0.0004 Å
• b: 21.2931 ± 0.0007 Å
• c: 18.7423 ± 0.0006 Å
• α: 90°
• β: 97.586 ± 0.0019°
• γ: 90°
• Cell volume: 5272.8 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.052
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.0968
• Weighted residual factors for all reflections included in the refinement: 0.1015
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No