Information card for entry 7020900

Structure parameters

• Formula: C8 H27 Ge La N6 S4
• Calculated formula: C8 H27 Ge La N6 S4
• Title of publication: The first examples of thiogermanate anion [GeS(3)(SH)](3-) as a bridging ligand to a lanthanide complex.
• Authors of publication: Zhou, Jian; Li, Rong; Ling, Xing; Chen, Rong; Hu, Feilong; Zeng, Yanfang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 6
• Pages of publication: 1961 - 1964
• a: 27.837 ± 0.006 Å
• b: 16.993 ± 0.003 Å
• c: 8.3185 ± 0.0017 Å
• α: 90°
• β: 103.96 ± 0.03°
• γ: 90°
• Cell volume: 3818.7 ± 1.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0254
• Residual factor for significantly intense reflections: 0.023
• Weighted residual factors for significantly intense reflections: 0.0564
• Weighted residual factors for all reflections included in the refinement: 0.0575
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No