Information card for entry 7020956

Structure parameters

• Common name: (C18MIm)3(Al2F9)(CH2Cl2)1.754
• Formula: C67.75 H132.51 Al2 Cl3.51 F9 N6
• Calculated formula: C67.754 H132.508 Al2 Cl3.508 F9 N6
• Title of publication: The first crystallographic example of a face-sharing fluoroaluminate anion Al(2)F(9)(3-).
• Authors of publication: Xu, Fei; Matsumoto, Kazuhiko; Hagiwara, Rika
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 6
• Pages of publication: 1965 - 1968
• a: 8.8125 ± 0.0006 Å
• b: 14.8052 ± 0.001 Å
• c: 30.847 ± 0.002 Å
• α: 96.083 ± 0.002°
• β: 99.426 ± 0.002°
• γ: 90.012 ± 0.002°
• Cell volume: 3947.3 ± 0.5 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.136
• Residual factor for significantly intense reflections: 0.0702
• Weighted residual factors for significantly intense reflections: 0.1752
• Weighted residual factors for all reflections included in the refinement: 0.2097
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No