Information card for entry 7021018

Structure parameters

• Formula: C186 H144 Cu6 N24 O18
• Calculated formula: C186 H144 Cu6 N24 O18
• Title of publication: Syntheses, structure diversity and properties of complexes with 4-acyl pyrazolone salicylidene hydrazide derivatives.
• Authors of publication: Zhang, Li; Xu, Guan-Cheng; Yang, Yun; Guo, Ji-Xi; Jia, Dian-Zeng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 12
• Pages of publication: 4248 - 4257
• a: 32.466 ± 0.003 Å
• b: 32.466 ± 0.003 Å
• c: 13.2855 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 12127 ± 2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0854
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for significantly intense reflections: 0.1421
• Weighted residual factors for all reflections included in the refinement: 0.1563
• Goodness-of-fit parameter for all reflections included in the refinement: 0.929
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No