Information card for entry 7021130
| Formula |
C61.5 H88 Cl5 N2 P Pd |
| Calculated formula |
C61.5 H88 Cl5 N2 P Pd |
| Title of publication |
Mixed phosphine/N-heterocyclic carbene palladium complexes: synthesis, characterization and catalytic use in aqueous Suzuki-Miyaura reactions. |
| Authors of publication |
Schmid, Thibault E.; Jones, Dale C.; Songis, Olivier; Diebolt, Olivier; Furst, Marc R. L.; Slawin, Alexandra M. Z.; Cazin, Catherine S. J. |
| Journal of publication |
Dalton transactions (Cambridge, England : 2003) |
| Year of publication |
2013 |
| Journal volume |
42 |
| Journal issue |
20 |
| Pages of publication |
7345 - 7353 |
| a |
12.32 ± 0.003 Å |
| b |
12.759 ± 0.002 Å |
| c |
21.547 ± 0.005 Å |
| α |
103.505 ± 0.008° |
| β |
104.578 ± 0.007° |
| γ |
93.875 ± 0.009° |
| Cell volume |
3158.4 ± 1.2 Å3 |
| Cell temperature |
93 ± 2 K |
| Ambient diffraction temperature |
93 ± 2 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0913 |
| Residual factor for significantly intense reflections |
0.0808 |
| Weighted residual factors for significantly intense reflections |
0.2344 |
| Weighted residual factors for all reflections included in the refinement |
0.2451 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.045 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/7021130.html
