Information card for entry 7021137

Structure parameters

• Formula: C32 H34 Ag2 F12 N8 O P2 S
• Calculated formula: C32 H34 Ag2 F12 N8 O P2 S
• Title of publication: Synthesis of polynuclear Ag(i) and Au(i) complexes from macrocyclic tetraimidazolium salts.
• Authors of publication: Schulte To Brinke, Christian; Pape, Tania; Hahn, F. Ekkehardt
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 20
• Pages of publication: 7330 - 7337
• a: 11.1472 ± 0.0006 Å
• b: 14.5134 ± 0.0007 Å
• c: 31.8567 ± 0.0012 Å
• α: 90°
• β: 99.567 ± 0.003°
• γ: 90°
• Cell volume: 5082.2 ± 0.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.087
• Residual factor for significantly intense reflections: 0.0744
• Weighted residual factors for significantly intense reflections: 0.1988
• Weighted residual factors for all reflections included in the refinement: 0.2119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No